Comprehensive Dataset on Rock-Fluid Interactions in Caney Shale (Project-FE0031776)_Task3

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This combined dataset comprises results from six distinct experimental studies focused on understanding the interactions between Caney Shale rock samples and various fluids under simulated reservoir conditions. These experiments provide critical insights into geochemical reactions, mineralogical transformations, and mechanical property changes. The datasets collectively support the evaluation of fluid-rock interaction mechanisms, offering valuable data for geochemical modeling and reservoir optimization. 1. Single-Component Hydraulic Fracturing Fluids This dataset contains results from experiments investigating the interactions between powdered Caney Shale rock samples and single-component hydraulic fracturing fluids. The primary focus was on understanding geochemical reactions during shut-in periods in hydraulic fracturing operations. 2. Field Fracturing Fluids This dataset evaluates the geochemical interactions between powdered Caney Shale rock samples and field fracturing fluids. The study examines changes in mineralogy and aqueous chemistry under controlled conditions simulating reservoir environments. 3. Field-Produced Brine This dataset documents experiments analyzing the interaction between powdered rock samples and field-produced brine. The study replicates subsurface reservoir conditions to investigate geochemical reactions and their implications for permeability and mineralogical changes. 4. Polished Shale and Field Fracturing Fluids This dataset includes experimental data from static batch experiments involving polished shale rock samples and field fracturing fluids. The experiments focused on microstructural, elemental, and hardness changes in rocks, as well as elemental and pH variations in reacted fluids. 5. Polished Shale and Produced Brine This dataset provides results from static batch reactor studies on polished shale rock samples interacting with untreated produced brine. Experiments explored variations in rock orientation relative to bedding planes under elevated temperature conditions, using methods like SEM, elemental mapping, hardness testing, and ICP-MS analysis. 6. Dynamic Core-Flooding with Fracturing Fluids This dataset presents results from dynamic core-flooding experiments on Caney Shale rock and fluid samples. The study investigates interactions between fracturing fluid and fractured rock surfaces under simulated reservoir conditions, with pre- and post-experiment evaluations of physical, chemical, and mechanical changes.

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1.	Awejori, G.A., Dong, W., Doughty, C., Spycher, N., Radonjic, M. (2024). Mineral and fluid transformation of hydraulically fractured shale: case study of Caney Shale in Southern Oklahoma. Geomechanics and Geophysics for Geo-Energy and Geo-Resources, 10(1), 128. 
2.	Awejori, G.A., Dong, W., Doughty, C., Spycher, N., Radonjic, M. (2024). Mineralogy and reactive fluid chemistry evolution of hydraulically fractured Caney Shale of Southern Oklahoma. Gas Science and Engineering, 131, 205458. https://doi.org/https://doi.org/10.1016/j.jgsce.2024.205458 
3.	Xiong, F., Wang, Y., Puckette, J., Grammer, M., Awejori, G.A., Radonjic, M. (2024). Geochemical and Microstructural Characterization of Shale Rock: A Workflow for Site Evaluation for Energy–Fluids Storage. Energy and Fuels. https://doi.org/10.1021/acs.energyfuels.4c03197 
4.	Awejori, G.A., Doughty, C., Xiong, F., Paronish, T., Spycher, N., Radonjic, M. (2022). Integrated experimental and modeling study of geochemical reactions of simple fracturing fluids with Caney Shale. Energy Fuels 36, 17, 10064–10081. 
5. 	Awejori, G.A., and Radonjic M. (2021). Review of Geochemical and Geo-mechanical Impact of Formation Clay-Fluid Interactions: Focus on Hydraulic Fracturing. IntechOpen.
6.	Awejori, G.A., Nyavor, P.A., Dong, W., Doughty, C., Rutqvist, J., Radonjic, M. (In Press). Geo-Mechanical and Geochemical Induced Fracture Closure in Hydraulically Fractured Caney Shale of Southern Oklahoma. The 4th International Conference on Coupled Processes in Fractured Geological Media. Yasuhara and Hashimoto (Eds). Kyoto, Japan.
7.	Awejori, G.A., Dong, W., Doughty, C., Radonjic, M. (2024). Geochemically driven Petrophysical Transformations in Caney Shale and its Impact on Reservoir Productivity. Unconventional Resources Technology Conference 2024. Houston, TX. 
8.	Xiong, F., Awejori, G.A., Radonjic, M. (2024). Effects of interactions between produced formation fluid and rock matrix on pore structure of Caney Shale, southern Oklahoma. 58th American Rock Mechanics Association (ARMA) Conference 2024. Golden, CO. 
9.	Dje, L.B., Awejori G.A., and Radonjic M. (2024). Comparison of Geochemical Reactivity of Marcellus and Caney shale based on effluent analysis. 58th American Rock Mechanics Association (ARMA) Conference 2024. Golden, CO. 
10.	Awejori, G.A., Xiong, F., Massion, C., Radonjic, M. (2023). Geochemical, Geo-mechanical, and Petrophysical Studies of Impacts of Rock-Fluid Interactions in Caney Formation in South Central Oklahoma. 57th American Rock Mechanics Association Symposium. Atlanta, GA.
11.	Katende, A., Awejori, G.A., Benge, M., Nakagawa, S., Wang, Y., Xiong, F., Puckette, J., Grammer, Rutqvist, J., Doughty, C., M., Bunger, A., Paronish, T., Crandall, D., Renk, J., and Radonjic, M. (2023). Multidimensional, experimental, and modeling evaluation of permeability evolution, the Caney Shale Field Lab, OK, USA. Unconventional Resources Technology Conference, Denver, CO. 
12.	Awejori, G.A., Whitworth, L., Paronish, T., Xiong, F., Katende, A., Radonjic, M. (2022). Fluid Induced Elemental and Mineralogy Alterations of Caney Shale. American Rock Mechanics Association Conference (ARMA), Santa Fe, NM. 
13.	Katende, A., Allen, C., Massion, C., Awejori, G.A., Xiong, F., Rutqvist, J., Nakagawa, S., Radonjic. M. (2022). Experiments and modeling of proppant embedment and fracture conductivity for the Caney Shale, Oklahoma, USA. American Rock Mechanics Association Conference (ARMA), Santa Fe, NM. 
14.	Awejori, G.A., Barnett, L., Al Dushaishi, M.F., Massion, C., Radonjic, M. (2022). Chemical and Mechanical Stability of Cement during Fluid Invasion in Hydraulic Fractured Geothermal Wells. Geothermal Rising Conference (GRC), Reno, NV. 
15.	Awejori, G.A., Jupudi, H., Massion, C., Radonjic, M. (2022). Study on Advanced Cementing Practices using Inert Graphene Nanoplatelets and Hydraulic Fracturing Fluids for Wellbore Integrity and Sustainability. The Minerals, Metals and Materials Society, TMS 2023 152nd Annual Meeting & Exhibition Supplemental Proceedings, The Minerals, Metals and Materials Series.
16.	Awejori, G.A., Luo, G., Grider, C., Katende, A., Radonjic, M. Doughty, C., Spycher, N. Paronish, T. O’Connell, L. Rihn, A. (2021). Fracturing Fluid-Induced Mineralogy Changes and Impact on Elastic Properties for the Caney Shale, Oklahoma. American Rock Mechanics Association (ARMA). Houston, Texas.

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Field	Value
Last Updated	December 21, 2024, 11:01 (LMT)
Created	December 20, 2024, 23:13 (LMT)
AI/ML Product	no
Citation	1. Awejori, G.A., Dong, W., Doughty, C., Spycher, N., Radonjic, M. (2024). Mineral and fluid transformation of hydraulically fractured shale: case study of Caney Shale in Southern Oklahoma. Geomechanics and Geophysics for Geo-Energy and Geo-Resources, 10(1), 128. 2. Awejori, G.A., Dong, W., Doughty, C., Spycher, N., Radonjic, M. (2024). Mineralogy and reactive fluid chemistry evolution of hydraulically fractured Caney Shale of Southern Oklahoma. Gas Science and Engineering, 131, 205458. https://doi.org/https://doi.org/10.1016/j.jgsce.2024.205458 3. Xiong, F., Wang, Y., Puckette, J., Grammer, M., Awejori, G.A., Radonjic, M. (2024). Geochemical and Microstructural Characterization of Shale Rock: A Workflow for Site Evaluation for Energy–Fluids Storage. Energy and Fuels. https://doi.org/10.1021/acs.energyfuels.4c03197 4. Awejori, G.A., Doughty, C., Xiong, F., Paronish, T., Spycher, N., Radonjic, M. (2022). Integrated experimental and modeling study of geochemical reactions of simple fracturing fluids with Caney Shale. Energy Fuels 36, 17, 10064–10081. 5. Awejori, G.A., and Radonjic M. (2021). Review of Geochemical and Geo-mechanical Impact of Formation Clay-Fluid Interactions: Focus on Hydraulic Fracturing. IntechOpen. 6. Awejori, G.A., Nyavor, P.A., Dong, W., Doughty, C., Rutqvist, J., Radonjic, M. (In Press). Geo-Mechanical and Geochemical Induced Fracture Closure in Hydraulically Fractured Caney Shale of Southern Oklahoma. The 4th International Conference on Coupled Processes in Fractured Geological Media. Yasuhara and Hashimoto (Eds). Kyoto, Japan. 7. Awejori, G.A., Dong, W., Doughty, C., Radonjic, M. (2024). Geochemically driven Petrophysical Transformations in Caney Shale and its Impact on Reservoir Productivity. Unconventional Resources Technology Conference 2024. Houston, TX. 8. Xiong, F., Awejori, G.A., Radonjic, M. (2024). Effects of interactions between produced formation fluid and rock matrix on pore structure of Caney Shale, southern Oklahoma. 58th American Rock Mechanics Association (ARMA) Conference 2024. Golden, CO. 9. Dje, L.B., Awejori G.A., and Radonjic M. (2024). Comparison of Geochemical Reactivity of Marcellus and Caney shale based on effluent analysis. 58th American Rock Mechanics Association (ARMA) Conference 2024. Golden, CO. 10. Awejori, G.A., Xiong, F., Massion, C., Radonjic, M. (2023). Geochemical, Geo-mechanical, and Petrophysical Studies of Impacts of Rock-Fluid Interactions in Caney Formation in South Central Oklahoma. 57th American Rock Mechanics Association Symposium. Atlanta, GA. 11. Katende, A., Awejori, G.A., Benge, M., Nakagawa, S., Wang, Y., Xiong, F., Puckette, J., Grammer, Rutqvist, J., Doughty, C., M., Bunger, A., Paronish, T., Crandall, D., Renk, J., and Radonjic, M. (2023). Multidimensional, experimental, and modeling evaluation of permeability evolution, the Caney Shale Field Lab, OK, USA. Unconventional Resources Technology Conference, Denver, CO. 12. Awejori, G.A., Whitworth, L., Paronish, T., Xiong, F., Katende, A., Radonjic, M. (2022). Fluid Induced Elemental and Mineralogy Alterations of Caney Shale. American Rock Mechanics Association Conference (ARMA), Santa Fe, NM. 13. Katende, A., Allen, C., Massion, C., Awejori, G.A., Xiong, F., Rutqvist, J., Nakagawa, S., Radonjic. M. (2022). Experiments and modeling of proppant embedment and fracture conductivity for the Caney Shale, Oklahoma, USA. American Rock Mechanics Association Conference (ARMA), Santa Fe, NM. 14. Awejori, G.A., Barnett, L., Al Dushaishi, M.F., Massion, C., Radonjic, M. (2022). Chemical and Mechanical Stability of Cement during Fluid Invasion in Hydraulic Fractured Geothermal Wells. Geothermal Rising Conference (GRC), Reno, NV. 15. Awejori, G.A., Jupudi, H., Massion, C., Radonjic, M. (2022). Study on Advanced Cementing Practices using Inert Graphene Nanoplatelets and Hydraulic Fracturing Fluids for Wellbore Integrity and Sustainability. The Minerals, Metals and Materials Society, TMS 2023 152nd Annual Meeting & Exhibition Supplemental Proceedings, The Minerals, Metals and Materials Series. 16. Awejori, G.A., Luo, G., Grider, C., Katende, A., Radonjic, M. Doughty, C., Spycher, N. Paronish, T. O’Connell, L. Rihn, A. (2021). Fracturing Fluid-Induced Mineralogy Changes and Impact on Elastic Properties for the Caney Shale, Oklahoma. American Rock Mechanics Association (ARMA). Houston, Texas.
Geospatial	no
Netl Product	yes
Poc Email	joseph.renk@netl.doe.gov
Point Of Contact	Joseph Renk
Program Or Project	Field Evaluation of the Caney Shale as an Emerging Unconventional Play, Southern Oklahoma
Project Number	FE0031776