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High temperature creep of refractory bricks. Final report

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The uniaxial compressive creep of the 13 high chromia-commercial refractories that are candidate materials for lining coal gasification vessels was studied using stresses from 50 to 1500 psi (0.34 MPa to 10.3 MPa) and temperature from 1900{degrees}F to 2600{degrees}F (1038{degrees} to 1427{degrees}C). The regimes to stress and temperature in which creep was active varied widely, depending on impurities and microstructure, not chromia content, and was active at lower stresses and temperatures than would be expected from hot strength data. The creep was always primary, going through steady state to failure as a transient phase. One specimen with a liquid phase at temperature gave a longer steady-state region. The primary creep time exponent varied from 0.4 to nearly one. It was smaller at low stresses and temperatures, but was often a linear function of stress. Activation enthalpies were less for refractories containing a significant liquid phase at temperature, and were in the range expected for cation diffusion. Current theoretical models to not fit these systems. Two models are suggested to explain the primary creep regime. More research to correlate primary creep with microstructure is needed.

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Last Updated September 29, 2016, 16:44 (LMT)
Created September 29, 2016, 16:44 (LMT)
Citation McGee, T.D. [Ames Lab., IA (United States)] ---- Roy Long, High temperature creep of refractory bricks. Final report, 2016-09-29, https://edx.netl.doe.gov/dataset/high-temperature-creep-of-refractory-bricks-final-report
Netl Product yes
Poc Email Roy.long@netl.doe.gov
Point Of Contact Roy Long
Program Or Project KMD
Publication Date 1991-5-15